반응식
[Br:1][C:2]1[CH:3]=[C:4]2[C:12](=[CH:13][CH:14]=1)[NH:11][C:10]1[CH:9]([NH2:15])[CH2:8][CH2:7][CH2:6][C:5]2=1.[CH3:16][N:17]([CH3:27])[C:18]1[CH:23]=[CH:22][C:21]([N:24]=[C:25]=[O:26])=[CH:20][CH:19]=1>>[Br:1][C:2]1[CH:3]=[C:4]2[C:12](=[CH:13][CH:14]=1)[NH:11][C:10]1[CH:9]([NH:15][C:25]([NH:24][C:21]3[CH:22]=[CH:23][C:18]([N:17]([CH3:27])[CH3:16])=[CH:19][CH:20]=3)=[O:26])[CH2:8][CH2:7][CH2:6][C:5]2=1참가 물질
3
실험 절차
N-(6-Bromo-2,3,4,9-tetrahydro-1H-carbazol-1-yl)-N′-[4-(dimethylamino)phenyl]urea was prepared from 6-bromo-2,3,4,9-tetrahydro-1H-carbazol-1-amine and 4-dimethylamino phenyl isocyanate in a similar manner as described above to give a tan solid (40% yield). 1H-NMR (DMSO-d6): δ 10.99 (s, 1H), 7.98 (s, 1H), 7.60 (d, 1H), 7.33-7.23 (m, 3H), 7.17 (dd, 1H), 6.71 (d, 2H), 6.44 (d, 1H), 5.00 (m, 1H), 2.84 (s, 6H), 2.67 (m, 2H), 2.04 (m, 1H), 1.94-1.74 (m, 3H); MS m/z 427 (M−1).
출처 및 근거
- ORD 기록
- ord-fb607263e894452a9a4c3aef4d7b0b66
- 출처 데이터셋
- uspto-grants-2008_09
- 특허 번호
- US07419997B2
연결된 노트
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