Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Guanidine → N-diaminomethylene-3-methylsulfonyl-4-(1-cyclopenten-3-yl)benzamide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Guanidine | HCID 3520 | — |
| 반응물 | 3-Methylsulfonyl-4-(1-cyclopenten-3-yl)-benzoyl chloride | HCID 19688268 | — |
| 생성물 | N-diaminomethylene-3-methylsulfonyl-4-(1-cyclopenten-3-yl)benzamide | HCID 19688175 | — |
반응 단계
Analogously to Example 1, by reaction of 2.2 g of 3-methylsulfonyl-4-(1-cyclopenten-3-yl)-benzoyl chloride with guanidine, customary working up gives N-diaminomethylene-3-methylsulfonyl-4-(1-cyclopenten-3-yl)benzamide, which can be recrystallized from acetonitrile/diethylether, m.p. 188°-190°.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05731351 |
| 출처 데이터셋 | uspto-grants-1998_03 |
| ORD ID | ord-90f641ecf797467592f5799ba146037c |
| 출처 메모 | uspto-grants-1998_03 |