Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Water → N-cyclohexylidene-2,6-dimethoxy-4-methylaniline
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Water | HCID 962 | — |
| 반응물 | Cyclohexanone | HCID 7967 | — |
| 반응물 | 2,6-Dimethoxy-4-methylaniline | HCID 12409090 | — |
| 용매 | Toluene | HCID 1140 | — |
| 생성물 | N-cyclohexylidene-2,6-dimethoxy-4-methylaniline | HCID 18936522 | — |
반응 단계
4.2 g of 2,6-dimethoxy-4-methylaniline are dissolved in 50 ml of toluene, 2.45 g of cyclohexanone are then added and the reaction mixture is heated at reflux for 18 hours. The water which is formed is removed as it is formed in the reaction mixture using a Dean and Stark apparatus. The toluene is evaporated and the oily N-cyclohexylidene-2,6-dimethoxy-4-methylaniline residue obtained is used without addition of purification in the following stage.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05731340 |
| 출처 데이터셋 | uspto-grants-1998_03 |
| ORD ID | ord-7722dbce85914723bdf979fd6d719ccd |
| 출처 메모 | uspto-grants-1998_03 |