참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | 4-Nitro-1,1'-biphenyl | HCID 7114 | — |
| 반응물 | Chlorosulfonic acid | HCID 24638 | — |
| 용매 | Chloroform | HCID 6212 | — |
| 생성물 | 4-Nitrobiphenylsulfonic acid | HCID 86599025 | 61% |
반응 단계
To a stirred solution of 4-nitrobiphenyl (50.00 g, 0.25 mol) in chloroform (750 mL) was added dropwise at room temperature chlorosulfonic acid (17 mL, 0.3 mol). The reaction mixture was stirred at 60° C. for 6 h. The white precipitate formed was collected by filtration and washed with cold chloroform. The product was air dried to give 31.00 g of 4-nitrobiphenylsulfonic acid (Yield 61%).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US07420001B2 |
|---|
| 출처 데이터셋 | uspto-grants-2008_09 |
|---|
| ORD ID | ord-26444b97df234c98a762ba056033954a |
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| 출처 메모 | uspto-grants-2008_09 |
|---|
