Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
2-Phenylisobutyric acid → 2-Methyl-2-phenylpropanoyl chloride
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 2-Phenylisobutyric acid | HCID 13222 | — |
| 반응물 | Oxalyl chloride | HCID 65578 | — |
| 용매 | Dichloromethane | HCID 6344 | — |
| 생성물 | 2-Methyl-2-phenylpropanoyl chloride | HCID 12369086 | — |
반응 단계
A solution of 2-Methyl-2-phenylpropionic acid (10 mmol, 1.0 eq.) and oxalyl chloride (40 mmol, 4.0 eq.) in dichloromethane (30 mL) was stirred at room temperature for 18 h. The mixture was concentrated in vacuo to afford the title compound as a yellow oil.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07420055B2 |
| 출처 데이터셋 | uspto-grants-2008_09 |
| ORD ID | ord-b388f55835f0450eb8040b6671d8a7a3 |
| 출처 메모 | uspto-grants-2008_09 |