돌아가기
Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HRID 2953생성일: 2026년 10월 24일

Water → 2-(1,1-Dimethylethyl)phenoxypropene

https://huagongshe.com/ko/reaction/2953

반응식

참여 물질

역할이름HCID투입량
반응물WaterHCID 962—
반응물2-Tert-ButylphenolHCID 6923—
반응물Allyl bromideHCID 7841—
반응물Potassium CarbonateHCID 11430—
용매AcetoneHCID 180—
생성물2-(1,1-Dimethylethyl)phenoxypropeneHCID 67631224—

반응 조건

온도35 °C

반응 단계

Allyl bromide (69.2 ml), 2-t-butylphenol (122.9 ml) and potassium carbonate (121.6 g) were stirred in 265 ml of acetone at reflux temperature for 50 hours and then cooled to 35° C. Water (600 ml) was added and the resulting layers were separated. The aqueous layer was extracted with 600 ml of diethyl ether. The organic layer was combined with the aqueous layer's ether extract and the resulting solution was dried over sodium sulfate overnight. After sodium sulfate removal, the solvent was evaporated to provide, after further workup, 147 g of the subtitled intermediate.

출처 및 근거

DOI10.6084/m9.figshare.5104873.v1
특허 번호US05731336
출처 데이터셋uspto-grants-1998_03
ORD IDord-f43f465340624f4daaa306b11664c6ec
출처 메모uspto-grants-1998_03