참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | 1,3-Dibromopropane | HCID 8001 | — |
| 반응물 | Diisopropylethylamine | HCID 81531 | — |
| 반응물 | Dimethyl Iminodiacetate Hydrochloride | HCID 2727727 | — |
| 용매 | Toluene | HCID 1140 | — |
| 생성물 | Dimethyl N-(3-Bromopropyl)iminodiacetate | HCID 19688438 | — |
반응 단계
A mixture of 1 mmol iminodiacetic acid dimethylester hydrochloride salt, 5 mmol N,N-diisopropyl-ethylamine and 3 mmol 1,3-dibromopropane in 2 mL toluene was stirred at 90° C. for 16 h and then chromatographed to provide the title compound as an oil.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US05731432 |
|---|
| 출처 데이터셋 | uspto-grants-1998_03 |
|---|
| ORD ID | ord-53859d19f5084c73a9229630dac0c84d |
|---|
| 출처 메모 | uspto-grants-1998_03 |
|---|
