Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
4-Toluenesulfonyl chloride → 3-iodo-N,4-dimethylbenzamide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 4-Toluenesulfonyl chloride | HCID 7397 | — |
| 반응물 | 3-Iodo-4-methylbenzoic acid | HCID 621640 | — |
| 반응물 | Methylamine hydrochloride | HCID 6364545 | — |
| 생성물 | 3-iodo-N,4-dimethylbenzamide | HCID 19688440 | — |
반응 단계
A solution of 1.0 mmol of 3-iodo-4-methylbenzoic acid, 1.2 mmol of TsCl, and 25 mmol of Py was stirred for 3 h and then 5 mmol of methylamine hydrochloride was added and stirring continued for 5 h. Chromatography provided N-methyl-(3-iodo-4-methylphenyl)carboxamide.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05731432 |
| 출처 데이터셋 | uspto-grants-1998_03 |
| ORD ID | ord-d5a686fbf7b9481c9a917b96b78bc8ab |
| 출처 메모 | uspto-grants-1998_03 |