Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Benzoyl Peroxide → Ethyl 3-bromo-4-(bromomethyl)benzoate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Benzoyl Peroxide | HCID 7187 | — |
| 반응물 | N-bromobutanimide | HCID 67184 | — |
| 반응물 | Ethyl 3-bromo-4-methylbenzoate | HCID 14945865 | — |
| 용매 | Carbon Tetrachloride | HCID 5943 | — |
| 생성물 | Ethyl 3-bromo-4-(bromomethyl)benzoate | HCID 13877460 | — |
반응 단계
A mixture of 1.0 mmol of ethyl 3-bromo-4-methylbenzoate, 1.0 mmol NBS, and 0.02 mmol benzoyl peroxide in 5 mL CCl4 was refluxed for 4 h and then processed by filtration and chromatography to provide ethyl 3-bromo-4-bromomethylbenzoate as an oil.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05731432 |
| 출처 데이터셋 | uspto-grants-1998_03 |
| ORD ID | ord-43fc139c41d84237a967f7fa62214d1c |
| 출처 메모 | uspto-grants-1998_03 |