참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Tributylvinyltin | HCID 81998 | — |
| 반응물 | Ethyl 3-(bromophenyl)acetate | HCID 11470552 | — |
| 촉매 | HCID 178418397 | HCID 178418397 | — |
| 용매 | Dimethylformamide | HCID 6228 | — |
| 생성물 | Ethyl 2-(3-vinylphenyl)acetate | HCID 11687033 | — |
반응 단계
A mixture of 1.0 mmol of ethyl 3-bromophenylacetate, 1.5 mmol of vinyltributyltin, and 0.1 mmol of Pd(PPh3)4 in 4 mL DMF was stirred and heated at 90° C. for 1-16 h. Chromatography provided ethyl 3-vinylphenylacetate.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US05731432 |
|---|
| 출처 데이터셋 | uspto-grants-1998_03 |
|---|
| ORD ID | ord-22f4a8336221412198601584d84cd4b1 |
|---|
| 출처 메모 | uspto-grants-1998_03 |
|---|
