3-Iodo-4-methylbenzyl alcohol → 3-Iodo-4-methylbenzaldehyde

HRID 2973

반응식

HRID 2973 반응식
[I:1][C:2]1[CH:3]=[C:4]([CH:7]=[CH:8][C:9]=1[CH3:10])[CH2:5][OH:6]>C(Cl)Cl.O=[Mn]=O>[I:1][C:2]1[CH:3]=[C:4]([CH:7]=[CH:8][C:9]=1[CH3:10])[CH:5]=[O:6]

참가 물질

4

반응물 1

HCID 51667983-Iodo-4-methylbenzyl alcohol

생성물 1

HCID 123302543-Iodo-4-methylbenzaldehyde

시약·촉매·용매 2

HCID 14801Manganese dioxide촉매HCID 6344Dichloromethane용매

실험 절차

A mixture of 1.0 mmol of this alcohol and 5.0 mmol of MnO2 in 5 mL of CH2Cl2 was stirred for 16 h at rt. Chromatography provided 3-iodo-4-methylbenzaldehyde.

출처 및 근거

ORD 기록
ord-bd82a5043a4441d6bb653b1731c79827
출처 데이터셋
uspto-grants-1998_03
특허 번호
US05731432

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