참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Triethylamine | HCID 8471 | — |
| 반응물 | p-Fluoronitrobenzene | HCID 9590 | — |
| 반응물 | 2,4-Dimethylbenzene-1,3-diamine | HCID 4625581 | — |
| 용매 | Dimethyl Sulfoxide | HCID 679 | — |
| 생성물 | 4-nitro-N-(3-{[(4-nitrophenyl)amino]methyl}benzyl)aniline | HCID 58794783 | — |
반응 단계
1.73 g of para-fluoronitrobenzene (2 eq.) were dissolved in 5 ml of DMSO. 1.2 equivalents of m-xylenediamine and 4 equivalents of triethylamine were added to the solution. The reaction mixture was heated at 60° C. for 20 hours. The mixture was then poured onto crushed ice and a precipitate formed. The latter was filtered, washed with water, and then dried.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US07422609B2 |
|---|
| 출처 데이터셋 | uspto-grants-2008_09 |
|---|
| ORD ID | ord-e6dc97c099be42f593855bc0cd045bfe |
|---|
| 출처 메모 | uspto-grants-2008_09 |
|---|
