Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Ethanol → N-(3-{[(4-aminophenyl)amino]methyl}benzyl)benzene-1,4-diamine tetrahydrochloride
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Ethanol | HCID 702 | — |
| 반응물 | Water | HCID 962 | — |
| 반응물 | Ammonium Chloride | HCID 25517 | — |
| 반응물 | 4-nitro-N-(3-{[(4-nitrophenyl)amino]methyl}benzyl)aniline | HCID 58794783 | — |
| 촉매 | Zinc | HCID 23994 | — |
| 용매 | N-methyl-2-pyrrolidone | HCID 13387 | — |
| 생성물 | N-(3-{[(4-aminophenyl)amino]methyl}benzyl)benzene-1,4-diamine tetrahydrochloride | HCID 69255182 | — |
반응 단계
The mixture of powdered zinc (30 g), ammonium chloride (3 g), water (5 ml) and absolute ethanol were brought to reflux with the oil bath. The 4-nitro-N-(3-{[(4-nitrophenyl)amino]methyl}benzyl)aniline (3 g) was dissolved in 50 ml of NMP and introduced dropwise until there was decoloration of the reaction medium, while at the same time the reflux was maintained.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07422609B2 |
| 출처 데이터셋 | uspto-grants-2008_09 |
| ORD ID | ord-6d2e4894e5894decb1f5ef3468560367 |
| 출처 메모 | uspto-grants-2008_09 |