Methylparaben → Methyl 4-(allyloxy)benzoate
반응식
[OH:1][C:2]1[CH:11]=[CH:10][C:5]([C:6]([O:8][CH3:9])=[O:7])=[CH:4][CH:3]=1.[CH2:12](Br)[CH:13]=[CH2:14].C([O-])([O-])=O.[K+].[K+]>CC(C)=O>[CH2:14]([O:1][C:2]1[CH:3]=[CH:4][C:5]([C:6]([O:8][CH3:9])=[O:7])=[CH:10][CH:11]=1)[CH:13]=[CH2:12]참가 물질
5
실험 절차
A mixture of 1.0 mmol of methyl 4-hydroxybenzoate, 2.0 mmol of allyl bromide, 5.0 mmol of K2CO3 in 2 mL of acetone was stirred for 16 h. Extraction provided methyl 4-allyloxybenzoate.
후처리
- extractionExtraction
출처 및 근거
- ORD 기록
- ord-136efa4c469642d7aa6076afa6f445aa
- 출처 데이터셋
- uspto-grants-1998_03
- 특허 번호
- US05731432
반응 노트
불러오는 중…