Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
4-Fluorobenzohydrazide → 4-Fluoro-benzoic acid-(1-imino-ethyl)-hydrazide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 4-Fluorobenzohydrazide | HCID 9972 | — |
| 반응물 | Ethanimidic acid, ethyl ester, hydrochloride (1:1) | HCID 2724290 | — |
| 생성물 | 4-Fluoro-benzoic acid-(1-imino-ethyl)-hydrazide | HCID 68492563 | — |
반응 단계
Prepared from 7.2 g (58 mmol) ethyl acetimidate hydrochloride and 5.00 g (32 mmol) 4-fluoro-benzoic acid hydrazide analogously to the method described for intermediate product la). Yield: 5.78 g (91%); mass spectroscopy [M+H]+=196.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07423036B2 |
| 출처 데이터셋 | uspto-grants-2008_09 |
| ORD ID | ord-b41695718a664a768a837ad4a3875418 |
| 출처 메모 | uspto-grants-2008_09 |