Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
5-Methyl-3-(4-trifluoromethylphenyl)-1H-[1,2,4]triazole → Tert-butyl {1,1-dimethyl-3-[5-methyl-3-(4-trifluoromethyl-phenyl)-[1,2,4]triazol-1-yl]-propyl}-carbamate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 5-Methyl-3-(4-trifluoromethylphenyl)-1H-[1,2,4]triazole | HCID 23228261 | — |
| 반응물 | tert-butyl N-(4-chloro-2-methylbutan-2-yl)carbamate | HCID 57429079 | — |
| 생성물 | Tert-butyl {1,1-dimethyl-3-[5-methyl-3-(4-trifluoromethyl-phenyl)-[1,2,4]triazol-1-yl]-propyl}-carbamate | HCID 86607261 | — |
반응 단계
The target compound is obtained analogously to the method described for intermediate product 1c) from 4.90 g (21.6 mmol) 5-methyl-3-(4-trifluoromethyl-phenyl)-1H-[1,2,4]triazol and 7.17 g (32.4 mmol) tert-butyl (3-chloro-1,1-dimethyl-propyl)-carbamate. White solid. Yield: 5.06 g (57%); mass spectroscopy [M+H]+=413.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07423036B2 |
| 출처 데이터셋 | uspto-grants-2008_09 |
| ORD ID | ord-f16bcecf67304ff280fcc11eb5d1c7d1 |
| 출처 메모 | uspto-grants-2008_09 |