Ethyl benzoylacetate → HCID 178515558, 화합물

HRID 29888

반응식

HRID 29888 반응식
C(O[C:4](=[O:14])[CH2:5][C:6](=O)[C:7]1[CH:12]=[CH:11][CH:10]=[CH:9][CH:8]=1)C.Cl.[Cl:16][C:17]1[CH:25]=[CH:24][C:20]([C:21]([NH2:23])=[NH:22])=[CH:19][CH:18]=1>>[Cl:16][C:17]1[CH:25]=[CH:24][C:20]([C:21]2[N:23]=[C:4]([OH:14])[CH:5]=[C:6]([C:7]3[CH:8]=[CH:9][CH:10]=[CH:11][CH:12]=3)[N:22]=2)=[CH:19][CH:18]=1

참가 물질

3

반응물 2

HCID 7170Ethyl benzoylacetateHCID 2034364-Chlorobenzene-1-carboximidamide hydrochloride

생성물 1

HCID 178515558HCID 178515558, 화합물

실험 절차

The title compound was prepared from 3-oxo-3-phenyl-propionic acid ethyl ester and 4-chloro-benzamidine hydrochloride according to general procedure 1. 1H NMR (DMSO-d6, 400 MHz) δ 6.97 (s, 1H), 7.50-7.58 (m, 3H), 7.16 (d, J=8.5 Hz, 2H), 8.10-8.20 (m, 2 H), 8.30 (d, J=8.5 Hz, 2H), 12.50 (br s, 1H); MS: m/z (ESI) 283 (M+H).

출처 및 근거

ORD 기록
ord-542fc9ecc55348e292c34758240a33d8
출처 데이터셋
uspto-grants-2008_09
특허 번호
US07423044B2

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