Ethyl benzoylacetate → HCID 178515559, 화합물

HRID 29890

반응식

HRID 29890 반응식
C(O[C:4](=[O:14])[CH2:5][C:6](=O)[C:7]1[CH:12]=[CH:11][CH:10]=[CH:9][CH:8]=1)C.Cl.[C:16]([NH2:24])(=[NH:23])[C:17]1[CH:22]=[CH:21][N:20]=[CH:19][CH:18]=1>>[C:7]1([C:6]2[N:24]=[C:16]([C:17]3[CH:22]=[CH:21][N:20]=[CH:19][CH:18]=3)[N:23]=[C:4]([OH:14])[CH:5]=2)[CH:8]=[CH:9][CH:10]=[CH:11][CH:12]=1

참가 물질

3

반응물 2

HCID 7170Ethyl benzoylacetateHCID 2776844Pyridine-4-amidine hydrochloride

생성물 1

HCID 178515559HCID 178515559, 화합물

실험 절차

The title compound was prepared from 3-oxo-3-phenyl-propionic acid ethyl ester and isonicotinamidine hydrochloride according to general procedure 1. 1H NMR (DMSO-d6, 400 MHz) δ 7.08 (s, 1H), 7.50-7.55 (m, 3H), 8.17-8.25 (m, 4 H), 8.88 (d, J=4.4 Hz, 2H), 10-12 (br s, 1H); MS: m/z(ESI) 250 (M+H).

출처 및 근거

ORD 기록
ord-655cf54f8f9d44f997d89b4fd30052d6
출처 데이터셋
uspto-grants-2008_09
특허 번호
US07423044B2

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