Ethyl benzoylacetate → HCID 178515556, 화합물

HRID 29891

반응식

HRID 29891 반응식
C(O[C:4](=[O:14])[CH2:5][C:6](=O)[C:7]1[CH:12]=[CH:11][CH:10]=[CH:9][CH:8]=1)C.Cl.[C:16]([NH2:24])(=[NH:23])[C:17]1[CH:22]=[CH:21][CH:20]=[CH:19][CH:18]=1>>[C:17]1([C:16]2[N:24]=[C:4]([OH:14])[CH:5]=[C:6]([C:7]3[CH:8]=[CH:9][CH:10]=[CH:11][CH:12]=3)[N:23]=2)[CH:22]=[CH:21][CH:20]=[CH:19][CH:18]=1

참가 물질

3

반응물 2

HCID 7170Ethyl benzoylacetateHCID 80289Benzamidine, hydrochloride

생성물 1

HCID 178515556HCID 178515556, 화합물

실험 절차

The title compound was prepared from 3-oxo-3-phenyl-propionic acid ethyl ester and benzamidine hydrochloride according to general procedure 1. 1H NMR (DMSO-d6, 400 MHz) δ 6.92 (s, 1H), 7.50-7.65 (m, 6H), 8.15-8.20 (m, 2H), 8.26 (d, J=7.2 Hz, 2H), 12.80 (br s, 1H); MS: m/z (ESI) 247 (M−H).

출처 및 근거

ORD 기록
ord-1d563964472e4576917b30ec19bdb230
출처 데이터셋
uspto-grants-2008_09
특허 번호
US07423044B2

연결된 노트

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