Ethyl isobutyrylacetate → HCID 178439458, 화합물

HRID 29893

반응식

HRID 29893 반응식
C(O[C:4](=[O:11])[CH2:5][C:6](=O)[CH:7]([CH3:9])[CH3:8])C.Cl.[Cl:13][C:14]1[CH:15]=[C:16]([CH:20]=[C:21]([Cl:23])[CH:22]=1)[C:17]([NH2:19])=[NH:18]>>[Cl:13][C:14]1[CH:15]=[C:16]([C:17]2[N:19]=[C:4]([OH:11])[CH:5]=[C:6]([CH:7]([CH3:8])[CH3:9])[N:18]=2)[CH:20]=[C:21]([Cl:23])[CH:22]=1

참가 물질

3

반응물 2

HCID 81583Ethyl isobutyrylacetateHCID 27431593,5-Dichlorobenzimidamide hydrochloride

생성물 1

HCID 178439458HCID 178439458, 화합물

실험 절차

The title compound was prepared from 4-methyl-3-oxo-pentanoic acid ethyl ester and 3,5-dichloro-benzamidine hydrochloride according to general procedure 1. 1H NMR (DMSO-d6, 400 MHz) δ 1.20-1.26 (m, 6H), 2.80-2.90 (m, 1H), 6.34 (s, 1H), 7.82(s, 1H), 8.18 (s, 2H), 12.50 (br s,1H); MS: m/z (ESI) 283 (M+H).

출처 및 근거

ORD 기록
ord-ca265c6ccff24dba8fa31f56fa64f6aa
출처 데이터셋
uspto-grants-2008_09
특허 번호
US07423044B2

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