참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Tyrosol | HCID 10393 | — |
| 반응물 | (Chloromethyl)cyclopropane | HCID 80013 | — |
| 반응물 | Potassium tert-butoxide | HCID 23665647 | — |
| 용매 | Dimethyl Sulfoxide | HCID 679 | — |
| 생성물 | 4-[2-(Cyclopropylmethoxy)ethyl]phenol | HCID 11052481 | — |
반응 단계
A reaction flask was charged with 4-Hydroxyphenethyl alcohol (1) (100 g, 0.72 mol), Potassium tert-butoxide (243 g, 2.17 mol), and 500 mL of DMSO. The mixture was stirred under nitrogen at 50° C. for 30 minutes. A solution of (Chloromethyl)cyclopropane (100 g, 1.10 mol) in 500 mL of DMSO was added dropwise to the reaction mixture. The mixture was then stirred at 50° C. for one hour and then cooled to room temperature.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US05731463 |
|---|
| 출처 데이터셋 | uspto-grants-1998_03 |
|---|
| ORD ID | ord-01039e4c25c144fb9c3dd548ff4937c0 |
|---|
| 출처 메모 | uspto-grants-1998_03 |
|---|
