2-Methoxybenzoyl chloride → 5-Methoxy-2-(2-methoxybenzoyl)benzoic acid

반응식

[CH3:1][O:2][C:3]1[CH:11]=[CH:10][CH:9]=[CH:8][C:4]=1[C:5](Cl)=[O:6].Br[C:13]1[CH:21]=[CH:20][C:19]([O:22][CH3:23])=[CH:18][C:14]=1[C:15]([OH:17])=[O:16]>>[CH3:23][O:22][C:19]1[CH:20]=[CH:21][C:13]([C:5](=[O:6])[C:4]2[CH:8]=[CH:9][CH:10]=[CH:11][C:3]=2[O:2][CH3:1])=[C:14]([CH:18]=1)[C:15]([OH:17])=[O:16]

참가 물질

반응물 2

HCID 889692-Methoxybenzoyl chloride

HCID 899062-Bromo-5-methoxybenzoic acid

생성물 1

HCID 692121735-Methoxy-2-(2-methoxybenzoyl)benzoic acid

실험 절차

This compound is obtained according to the procedure described in 1.1. by reacting 2-methoxybenzoyl chloride and 2-bromo-5-methoxybenzoic acid after halogen-lithium exchange. It is used in crude form in the following reaction.

후처리

customThis compound is obtained
customin the following reaction

출처 및 근거

ORD 기록: ord-af1c2500ef664f24b5977c2435c07292
출처 데이터셋: uspto-grants-2008_09
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US07423030B2

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