Veratroyl chloride → 2-(3,4-Dimethoxybenzoyl)-5-methoxybenzoic acid

반응식

[CH3:1][O:2][C:3]1[CH:4]=[C:5]([CH:9]=[CH:10][C:11]=1[O:12][CH3:13])[C:6](Cl)=[O:7].Br[C:15]1[CH:23]=[CH:22][C:21]([O:24][CH3:25])=[CH:20][C:16]=1[C:17]([OH:19])=[O:18]>>[CH3:1][O:2][C:3]1[CH:4]=[C:5]([CH:9]=[CH:10][C:11]=1[O:12][CH3:13])[C:6]([C:15]1[CH:23]=[CH:22][C:21]([O:24][CH3:25])=[CH:20][C:16]=1[C:17]([OH:19])=[O:18])=[O:7]

참가 물질

반응물 2

HCID 77070Veratroyl chloride

HCID 899062-Bromo-5-methoxybenzoic acid

생성물 1

HCID 692141502-(3,4-Dimethoxybenzoyl)-5-methoxybenzoic acid

실험 절차

This compound is obtained according to the procedure described in 1.1. by reacting 3,4-dimethoxybenzoyl chloride and 2-bromo-5-methoxybenzoic acid after halogen-lithium exchange. It is used in crude form in the following reaction.

후처리

customThis compound is obtained
customin the following reaction

출처 및 근거

ORD 기록: ord-e3960857a0f8439392478298ee564953
출처 데이터셋: uspto-grants-2008_09
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US07423030B2

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