Propionyl chloride → 3,5-Dimethoxy-2-propionylbenzoic acid

반응식

[CH3:1][O:2][C:3]1[CH:4]=[C:5]([CH:10]=[C:11]([O:13][CH3:14])[CH:12]=1)[C:6]([O:8]C)=[O:7].[C:15](Cl)(=[O:18])[CH2:16][CH3:17]>>[CH3:1][O:2][C:3]1[C:4]([C:15](=[O:18])[CH2:16][CH3:17])=[C:5]([CH:10]=[C:11]([O:13][CH3:14])[CH:12]=1)[C:6]([OH:8])=[O:7]

참가 물질

반응물 2

HCID 62324Propionyl chloride

HCID 75074Methyl 3,5-Dimethoxybenzoate

생성물 1

HCID 692142953,5-Dimethoxy-2-propionylbenzoic acid

실험 절차

This compound is synthesized by reacting methyl 3,5-dimethoxybenzoate with propionyl chloride via the Friedel-Crafts reaction, followed by saponification of the ester obtained, according to the method described in 2.1. It is used in crude form in the following reaction.

후처리

customThis compound is synthesized
customvia the Friedel-Crafts reaction
customobtained
customin the following reaction

출처 및 근거

ORD 기록: ord-9378b4ce2200480e812cad8e537d91d2
출처 데이터셋: uspto-grants-2008_09
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US07423030B2

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