1,3-Benzodioxole-5-carboxylic acid → 2-(1,3-Benzodioxol-5-yl)carbonyl-5-methoxybenzoic acid

반응식

[O:1]1[C:5]2[CH:6]=[CH:7][C:8]([C:10]([OH:12])=O)=[CH:9][C:4]=2[O:3][CH2:2]1.Br[C:14]1[CH:22]=[CH:21][C:20]([O:23][CH3:24])=[CH:19][C:15]=1[C:16]([OH:18])=[O:17]>>[O:1]1[C:5]2[CH:6]=[CH:7][C:8]([C:10]([C:14]3[CH:22]=[CH:21][C:20]([O:23][CH3:24])=[CH:19][C:15]=3[C:16]([OH:18])=[O:17])=[O:12])=[CH:9][C:4]=2[O:3][CH2:2]1

참가 물질

반응물 2

HCID 71961,3-Benzodioxole-5-carboxylic acid

HCID 899062-Bromo-5-methoxybenzoic acid

생성물 1

HCID 692130352-(1,3-Benzodioxol-5-yl)carbonyl-5-methoxybenzoic acid

실험 절차

This compound is obtained according to the procedure described in 1.1. by reacting 1,3-benzodioxole-5-carboxylic acid and 2-bromo-5-methoxybenzoic acid after halogen-lithium exchange. It is used in crude form in the following reaction.

후처리

customThis compound is obtained
customin the following reaction

출처 및 근거

ORD 기록: ord-dc7d7e77c3d84dba8b6509b0cf2ad35e
출처 데이터셋: uspto-grants-2008_09
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US07423030B2

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