2-Bromo-5-methoxybenzoic acid → 2-Acetyl-5-methoxybenzoic acid

HRID 30016

반응식

HRID 30016 반응식
Br[C:2]1[CH:10]=[CH:9][C:8]([O:11][CH3:12])=[CH:7][C:3]=1[C:4]([OH:6])=[O:5].C([Li])CCC.CON(C)[C:21](=[O:23])[CH3:22]>>[C:21]([C:2]1[CH:10]=[CH:9][C:8]([O:11][CH3:12])=[CH:7][C:3]=1[C:4]([OH:6])=[O:5])(=[O:23])[CH3:22]

참가 물질

4

반응물 3

HCID 899062-Bromo-5-methoxybenzoic acidHCID 537505N-Methoxy-N-methylacetamideHCID 178418339Butyllithium

생성물 1

HCID 201632832-Acetyl-5-methoxybenzoic acid

실험 절차

This compound is synthesized according to the method described in 3.2. by reacting 2-bromo-5-methoxybenzoic acid pretreated with n-butyllithium with N-methoxy-N-methylacetamide. It is used in crude form in the following reaction.

후처리

  1. customThis compound is synthesized
  2. customin the following reaction

출처 및 근거

ORD 기록
ord-919f3b533e4a42edb8eb1acaf06fb298
출처 데이터셋
uspto-grants-2008_09
특허 번호
US07423030B2

연결된 노트

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