Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
2-Bromo-5-methoxybenzoic acid → 5-Methoxy-2-pyridin-3-ylbenzoic acid
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 2-Bromo-5-methoxybenzoic acid | HCID 89906 | — |
| 반응물 | N-Methoxy-N-methylnicotinamide | HCID 10558996 | — |
| 반응물 | Butyllithium | HCID 178418339 | — |
| 생성물 | 5-Methoxy-2-pyridin-3-ylbenzoic acid | HCID 46315937 | — |
반응 단계
This compound is synthesized according to the method described in 3.2. by reacting 2-bromo-5-methoxybenzoic acid pretreated with n-butyllithium with N-methoxy-N-methylnicotinamide. After precipitation in aqueous phase at pH 4, followed by filtration and drying, a beige-coloured powder is obtained.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07423030B2 |
| 출처 데이터셋 | uspto-grants-2008_09 |
| ORD ID | ord-3ea30621b6904a65840e6a85fe72c5cc |
| 출처 메모 | uspto-grants-2008_09 |