Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
2-Naphthalenecarboxaldehyde → (3R)-1-(Naphthalen-2-ylmethyl)-3-tert-butyloxycarbonylaminopyrrolidine
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 2-Naphthalenecarboxaldehyde | HCID 6201 | — |
| 반응물 | (3R)-(+)-3-(tert-Butoxycarbonylamino)pyrrolidine | HCID 1514397 | — |
| 생성물 | (3R)-1-(Naphthalen-2-ylmethyl)-3-tert-butyloxycarbonylaminopyrrolidine | HCID 69215056 | — |
반응 단계
This compound was prepared via the reductive amination method described in 49.2, by reaction of (R)-3-tert-butyloxycarbonylaminopyrrolidine with 2-naphthaldehyde. The residue is purified on a column of silica (eluent: from 100/0 to 90/10 (v/v) dichloromethane/methanol).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07423030B2 |
| 출처 데이터셋 | uspto-grants-2008_09 |
| ORD ID | ord-a313387baa2843c19b9ac2231bc6885f |
| 출처 메모 | uspto-grants-2008_09 |