Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
4-Iodoanisole → (2-Amino-6-chloro-pyridin-3-yl)-(4-methoxy-phenyl)-methanone
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 4-Iodoanisole | HCID 69676 | — |
| 반응물 | 2-Amino-6-chloro-N-methoxy-N-methyl-nicotinamide | HCID 58590824 | — |
| 반응물 | HCID 178506735 | HCID 178506735 | — |
| 생성물 | (2-Amino-6-chloro-pyridin-3-yl)-(4-methoxy-phenyl)-methanone | HCID 58590836 | — |
반응 단계
The title compound was prepared from 2-Amino-6-chloro-N-methoxy-N-methyl-nicotinamide (Example 3) and 4-methoxyphenyllithium freshly prepared from 4-iodoanisole (Aldrich) using the procedure described in Example 7. HRMS, observed: 262.0512, Calcd for M+: 262.0509.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07423051B2 |
| 출처 데이터셋 | uspto-grants-2008_09 |
| ORD ID | ord-176c6c62ac88485a97538c505ba1b9d6 |
| 출처 메모 | uspto-grants-2008_09 |