Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
2-Thiophenecarboxaldehyde → Methyl 3-(thiophen-2-yl)acrylate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 2-Thiophenecarboxaldehyde | HCID 7364 | — |
| 반응물 | Nsc 634137 | HCID 184894 | — |
| 생성물 | Methyl 3-(thiophen-2-yl)acrylate | HCID 2778970 | 75% |
반응 단계
Thiophene-2-carbaldehyde (4.00 g, 35.7 mmol) and [bis-(2,2,2-trifluoro-ethoxy)-phosphoryl]-acetic acid methyl ester (12.5 g, 39.3 mmol) were treated by the method outlined in Example 34, step a to afford the subtitle compound (4.5 g, yield: 75%). MS calculated for C8H8O2S+H: 169, observed: 169.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07423056B2 |
| 출처 데이터셋 | uspto-grants-2008_09 |
| ORD ID | ord-af0c01bc0e364401b9be3bda4a583535 |
| 출처 메모 | uspto-grants-2008_09 |