Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
3-Bromoaniline → 3-(3-Bromophenylamino)-6-oxo-7-phenyl-6,7-dihydrothieno[2,3-b]pyridine-2-carbonitrile
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 3-Bromoaniline | HCID 11562 | — |
| 반응물 | 6-Oxo-7-phenyl-3-phenylamino-6,7-dihydro-thieno[2,3-b]pyridine-2-carbonitrile | HCID 68457647 | — |
| 생성물 | 3-(3-Bromophenylamino)-6-oxo-7-phenyl-6,7-dihydrothieno[2,3-b]pyridine-2-carbonitrile | HCID 68457032 | — |
반응 단계
The title compound was prepared from 3-bromoaniline (155 mg, 0.9 mmol) following the method described for the compound of Example 18 to give the product as a pale yellow solid (183 mg). δH (CDCl3) 7.91-7.83 (3H, m), 7.83-7.66 (2H, m), 7.62 (1H, d, J 9.7 Hz), 7.52-7.44 (3H, m), 7.23 (1H, dt, J 7.1, 1.7 Hz), 6.81 (1H, d, J 9.7 Hz), 6.74 (1H, bs). LCMS (ES+) 422 (M+H)+79Br, 424 (M+H)+81Br.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07423047B2 |
| 출처 데이터셋 | uspto-grants-2008_09 |
| ORD ID | ord-363133a50db34982b05909cec10d7b23 |
| 출처 메모 | uspto-grants-2008_09 |