Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Morpholine → 4-((5-Bromopyridin-3-yl)methyl)morpholine
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Morpholine | HCID 8083 | — |
| 반응물 | 5-Bromo-3-pyridinecarboxaldehyde | HCID 2784734 | — |
| 생성물 | 4-((5-Bromopyridin-3-yl)methyl)morpholine | HCID 22390415 | 61% |
반응 단계
The title compound was prepared in a similar way as described in Example 18, Step C, using 5-bromo-pyridine-3-carbaldehyde and morpholine. The crude compound was purified (SiO2: 0-3% 2 M NH3 in MeOH/DCM) to provide the title compound (61%).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07423147B2 |
| 출처 데이터셋 | uspto-grants-2008_09 |
| ORD ID | ord-fa162b65c69e4dc3b185bf027fd7d8b4 |
| 출처 메모 | uspto-grants-2008_09 |