Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Thiophosgene → HCID 178440816, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Thiophosgene | HCID 10040 | — |
| 반응물 | 3-tert-Butylaniline | HCID 79334 | — |
| 반응물 | Sodium Bicarbonate | HCID 516892 | — |
| 용매 | Acetone | HCID 180 | — |
| 생성물 | HCID 178440816 | HCID 178440816 | — |
반응 단계
To 3-(tert-butyl)phenylamine in acetone at 0° C. was added sodium bicarbonate (2 eq) and thiophosgene (2 eq). The mixture was brought to ambient temperature and concentrated and partitioned between ethyl acetate and water. The organic layer was dried with sodium bicarbonate and sodium sulfate and concentrated to yield 3-(tert-butyl)benzenisothiocyanate. MS: MH+=192.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07423150B2 |
| 출처 데이터셋 | uspto-grants-2008_09 |
| ORD ID | ord-5c2f9b6dcb724652b0a751510608c005 |
| 출처 메모 | uspto-grants-2008_09 |