Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Diethyl Sulfate → 2-Bromophenetole
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Diethyl Sulfate | HCID 6163 | — |
| 반응물 | 2-Bromophenol | HCID 7244 | — |
| 용매 | Sodium Hydroxide | HCID 14798 | — |
| 생성물 | 2-Bromophenetole | HCID 68500 | — |
반응 단계
A mixture of 17.5 g of 2-bromophenol, 66 ml of diethyl sulphate and 170 ml of 10% NaOH solution is refluxed for 2 hours. After cooling the reaction mixture to RT, it is extracted with EtOAc, the organic phase is washed with 2N NaOH solution and dried over Na2SO4, and the solvent is evaporated off under vacuum. 19.6 g of the expected product are obtained.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07425566B2 |
| 출처 데이터셋 | uspto-grants-2008_09 |
| ORD ID | ord-7430bb1eac354422a753a5f7420cbe7a |
| 출처 메모 | uspto-grants-2008_09 |