3-Allyl-4-hydroxybenzonitrile → 3-Allyl-4-benzyloxy-benzonitrile

HRID 31501노트

반응식

HRID 31501 반응식
[CH2:1]([C:4]1[CH:5]=[C:6]([CH:9]=[CH:10][C:11]=1[OH:12])[C:7]#[N:8])[CH:2]=[CH2:3].[CH2:13](Br)[C:14]1[CH:19]=[CH:18][CH:17]=[CH:16][CH:15]=1.C(=O)([O-])[O-].[K+].[K+]>CN(C)C=O>[CH2:1]([C:4]1[CH:5]=[C:6]([CH:9]=[CH:10][C:11]=1[O:12][CH2:13][C:14]1[CH:19]=[CH:18][CH:17]=[CH:16][CH:15]=1)[C:7]#[N:8])[CH:2]=[CH2:3]

참가 물질

4

반응물 2

HCID 2584423-Allyl-4-hydroxybenzonitrileHCID 86593042Benzylbromide potassium carbonate

생성물 1

HCID 114593413-Allyl-4-benzyloxy-benzonitrile

시약·촉매·용매 1

HCID 6228Dimethylformamide용매

실험 절차

Prepared analogously to Example 5d from 3-allyl-4-hydroxy-benzonitrile and benzylbromide/potassium carbonate in dimethylformamide.

출처 및 근거

ORD 기록
ord-ba07be39c12743f09d36ec0f4f56c48a
출처 데이터셋
uspto-grants-2008_09
특허 번호
US07425641B2

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