Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
5-Benzyloxy-2,2-dimethyl-1,3-dioxane → 2-(Phenylmethoxy)-1,3-propanediol
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 5-Benzyloxy-2,2-dimethyl-1,3-dioxane | HCID 20364889 | — |
| 용매 | Methanol | HCID 887 | — |
| 생성물 | 2-(Phenylmethoxy)-1,3-propanediol | HCID 203567 | 94% |
반응 단계
To a methanol (50 ml) solution of the 5-(benzyloxy)-2,2-dimethyl-1,3-dioxane (6.5 g, 29.2 mmol) obtained in the step (9b), DOWEX® 50W-X8 (5 g) was added and stirred at room temperature. After 2 hours, the reaction mixture was filtered and concentrated to obtain the title compound (5.0 g, 93.8%) as a colorless oil.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07425634B2 |
| 출처 데이터셋 | uspto-grants-2008_09 |
| ORD ID | ord-ec108d8ddcc040d39d8ce9b503d6cacb |
| 출처 메모 | uspto-grants-2008_09 |