Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Cyclobutanone → 2-(((4-(5,9-Dioxaspiro[3.5]non-7-ylmethoxy)-3-methylpyridin-2-yl)methyl)sulfinyl)-1h-benzimidazole sodium salt
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Cyclobutanone | HCID 14496 | — |
| 반응물 | Trimethylolmethane | HCID 78432 | — |
| 반응물 | 2-(((4-(6,10-Dioxaspiro[4.5]dec-8-ylmethoxy)-3-methylpyridin-2-yl)methyl)sulfinyl)-1h-benzimidazole sodium salt | HCID 66776670 | — |
| 생성물 | 2-(((4-(5,9-Dioxaspiro[3.5]non-7-ylmethoxy)-3-methylpyridin-2-yl)methyl)sulfinyl)-1h-benzimidazole sodium salt | HCID 66776535 | 6.2% |
반응 단계
The same procedure as in the steps (21a) and (21b) of Example 21 was repeated using 2-(hydroxymethyl)-1,3-propanediol and cyclobutanone to obtain the title compound (265 mg, total yield: 6.2%) as a light yellow solid.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07425634B2 |
| 출처 데이터셋 | uspto-grants-2008_09 |
| ORD ID | ord-ecc04e0b96ed41f99ab7ea4dcf8ab626 |
| 출처 메모 | uspto-grants-2008_09 |