Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
(2,2-Diethyl-1,3-dioxan-5-yl)methanol → 2-(((4-((2,2-Diethyl-1,3-dioxan-5-yl)methoxy)-3-methylpyridin-2-yl)methyl)sulfinyl)-1h-benzimidazole sodium salt
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | (2,2-Diethyl-1,3-dioxan-5-yl)methanol | HCID 14629254 | — |
| 반응물 | 2-(((4-((2-Methoxy-1,3-dioxan-5-yl)methoxy)-3-methylpyridin-2-yl)methyl)sulfinyl)-1h-benzimidazole sodium salt | HCID 66776002 | — |
| 생성물 | 2-(((4-((2,2-Diethyl-1,3-dioxan-5-yl)methoxy)-3-methylpyridin-2-yl)methyl)sulfinyl)-1h-benzimidazole sodium salt | HCID 66776679 | 9.7% |
반응 단계
The same procedure as in the steps (6b) to (6f) of Example 6 was repeated using (2,2-diethyl-1,3-dioxan-5-yl)methanol obtained in the step (23a) to obtain the title compound (164 mg, total yield: 9.7%) as a light yellow solid.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07425634B2 |
| 출처 데이터셋 | uspto-grants-2008_09 |
| ORD ID | ord-81a9d7e6c383445ba117fb9ce0154a93 |
| 출처 메모 | uspto-grants-2008_09 |