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Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HRID 31634생성일: 2026년 10월 25일

1,5-Dioxaspiro[5.5]undec-3-ylmethanol → 2-(((4-(1,5-Dioxaspiro[5.5]undec-3-ylmethoxy)-3-methylpyridin-2-yl)methyl)sulfinyl)-1h-benzimidazole sodium salt

https://huagongshe.com/reaction/31634

반응식

참여 물질

역할이름HCID투입량
반응물1,5-Dioxaspiro[5.5]undec-3-ylmethanolHCID 15286693—
반응물2-(((4-((2-Methoxy-1,3-dioxan-5-yl)methoxy)-3-methylpyridin-2-yl)methyl)sulfinyl)-1h-benzimidazole sodium saltHCID 66776002—
생성물2-(((4-(1,5-Dioxaspiro[5.5]undec-3-ylmethoxy)-3-methylpyridin-2-yl)methyl)sulfinyl)-1h-benzimidazole sodium saltHCID 667761048.4%

반응 단계

The same procedure as in the steps (6b) to (6f) of Example 6 was repeated using 1,5-dioxaspiro[5.5]undec-3-ylmethanol obtained in the step (25a) to obtain the title compound (125 mg, total yield: 8.4%) as a light yellow solid.

출처 및 근거

DOI10.6084/m9.figshare.5104873.v1
특허 번호US07425634B2
출처 데이터셋uspto-grants-2008_09
ORD IDord-0a3e81c78d194ef582f33088c3b45e53
출처 메모uspto-grants-2008_09