Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
4-Chloro-2,3,5-trimethyl-1-oxidopyridin-1-ium → 2-(((4-(1,4-Dioxan-2-ylmethoxy)-3,5-dimethylpyridin-2-yl)methyl)sulfinyl)-1h-benzimidazole sodium salt
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 4-Chloro-2,3,5-trimethyl-1-oxidopyridin-1-ium | HCID 2779141 | — |
| 반응물 | HCID 66776308 | HCID 66776308 | — |
| 생성물 | 2-(((4-(1,4-Dioxan-2-ylmethoxy)-3,5-dimethylpyridin-2-yl)methyl)sulfinyl)-1h-benzimidazole sodium salt | HCID 66776242 | 18% |
반응 단계
The same procedure as in the steps (62a) to (62d) of Example 62 was repeated using 4-chloro-2,3,5-trimethylpyridine 1-oxide to obtain the title compound (355 mg, total yield: 18%) as a white solid.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07425634B2 |
| 출처 데이터셋 | uspto-grants-2008_09 |
| ORD ID | ord-b5a50899ee1e4c739ff3100981252503 |
| 출처 메모 | uspto-grants-2008_09 |