Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Methylamine → 6-chloro-N-methyl-3-nitropyridin-2-amine
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Methylamine | HCID 6329 | — |
| 반응물 | 6-Chloro-2-dimethylamino-3-nitropyridine | HCID 21787625 | — |
| 생성물 | 6-chloro-N-methyl-3-nitropyridin-2-amine | HCID 10750094 | — |
반응 단계
6-chloro-2-methylamino-3-nitro-pyridine was prepared in accordance to the procedure described above for the preparation of 6-chloro-2-dimethylamino-3-nitro pyridine by using solution of methyl amine. The crude product was purified by flash chromatography, eluting with 90% hexane: 10% ethyl acetate to 16 (300 mg).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07425557B2 |
| 출처 데이터셋 | uspto-grants-2008_09 |
| ORD ID | ord-28a6a2630152406486bf79fccdaebfea |
| 출처 메모 | uspto-grants-2008_09 |