Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Water → N,N-bis[4''-(N-phenyl-1-naphthylamino)-p-terphenyl-4-yl]amine
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Water | HCID 962 | — |
| 반응물 | 1,2-Diethylbenzene | HCID 8657 | — |
| 반응물 | Potassium Hydroxide | HCID 14797 | — |
| 반응물 | N,N-bis[4''-(N-phenyl-1-naphthylamino)-p-terphenyl-4-yl]acetamide | HCID 59793205 | — |
| 용매 | Hexane | HCID 8058 | — |
| 생성물 | N,N-bis[4''-(N-phenyl-1-naphthylamino)-p-terphenyl-4-yl]amine | HCID 59793193 | 85.5% |
반응 단계
Charged were N,N-bis[4″-(N-phenyl-1-naphthylamino)-p-terphenyl-4-yl]acetamide 82.0 g, a 50% potassium hydroxide aqueous solution 39 g and diethylbenzene 100 ml, and the mixture was heated and refluxed for 3 days. After finishing the reaction, the mixture was left cooling down, and water 100 ml and hexane 500 ml were added thereto. The brown solid matter deposited was filtered off and dried under reduced pressure to obtain 67 g of N,N-bis[4″-(N-phenyl-1-naphthylamino)-p-terphenyl-4-yl]amine.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07425654B2 |
| 출처 데이터셋 | uspto-grants-2008_09 |
| ORD ID | ord-86bb213d299e42d6ac8e1d5218b776b3 |
| 출처 메모 | uspto-grants-2008_09 |