참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Dimethylalumanylium chloride | HCID 16686359 | — |
| 반응물 | Lithium pentamethylcyclopentadiene | HCID 67305831 | — |
| 용매 | Toluene | HCID 1140 | — |
| 생성물 | Dimethyl(pentamethylcyclopentadienyl)aluminum | HCID 16708437 | 78% |
반응 단계
1.14 g of lithium pentamethylcyclopentadiene (C5Me5Li) and 50 ml of toluene were added into a 100-ml Schlenk flask bottle at room temperature. Then 8 ml of dimethylaluminum chloride (1M in hexane) was added to the mixture. The mixture solution was heated at 80° C. for four hours. After the removal of LiCl, the filtrate was vacuum dried to obtain a yellowish dimethyl(pentamethylcyclopentadienyl)aluminum. The yield was 78%.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US06211106B1 |
|---|
| 출처 데이터셋 | uspto-grants-2001_04 |
|---|
| ORD ID | ord-4e0a52e81c3946bc92d8d6cbb03edb98 |
|---|
| 출처 메모 | uspto-grants-2001_04 |
|---|
