Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
2-(Benzyloxy)benzaldehyde → 1-(2-(Benzyloxy)phenyl)-2-propen-1-ol
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 2-(Benzyloxy)benzaldehyde | HCID 344784 | — |
| 반응물 | HCID 178418507 | HCID 178418507 | — |
| 용매 | Tetrahydrofuran | HCID 8028 | — |
| 생성물 | 1-(2-(Benzyloxy)phenyl)-2-propen-1-ol | HCID 22009001 | — |
반응 단계
2-(benzyloxy)benzaldehyde (5g, 23.6 mmol) was reacted with vinylmagnesium bromide in THF (90 ml) at 0 C. The reaction was quenched with 2 N HCl and the product was extracted in i-PrOAc, dried over Na2SO4 and purified by flash chromatography with EtOAc:toluene 2.5:97.5.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06211197B1 |
| 출처 데이터셋 | uspto-grants-2001_04 |
| ORD ID | ord-a4708b1709d247f8a0d9098dd75df039 |
| 출처 메모 | uspto-grants-2001_04 |