Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
1,3-Dichloroacetone → 2-(4-Benzyloxy-phenyl)-4-chloromethyl-oxazole
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 1,3-Dichloroacetone | HCID 10793 | — |
| 반응물 | 4-Benzyloxybenzamide | HCID 2726431 | — |
| 생성물 | 2-(4-Benzyloxy-phenyl)-4-chloromethyl-oxazole | HCID 22009845 | 33% |
반응 단계
In substantially the same manner as in Reference Example 31, 4-benzyloxybenzamide was allowed to react with 1,3-dichloroacetone to give 2-(4-benzyloxyphenyl)-4-chloromethyloxazole. The yield was 33%. Recrystallization from ethyl acetate-hexane gave colorless prisms, mp 119-120° C.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06211215B1 |
| 출처 데이터셋 | uspto-grants-2001_04 |
| ORD ID | ord-c866ceb1ade34cdda156129c141a786c |
| 출처 메모 | uspto-grants-2001_04 |