Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
1-[4-(3-Hydroxyphenyl)butyl]imidazole → HCID 22009687, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 1-[4-(3-Hydroxyphenyl)butyl]imidazole | HCID 22009661 | — |
| 반응물 | 5-Chloromethyl-2-(2-thienyl)benzoxazole | HCID 22009720 | — |
| 생성물 | HCID 22009687 | HCID 22009687 | 70% |
반응 단계
In substantially the same manner as in Working Example 72, 1-[4-(3-hydroxyphenyl)butyl]imidazole was allowed to react with 5-chloromethyl-2-(2-thienyl)benzoxazole to give 5-[3-[4-(1-imidazolyl)butyl]phenoxymethyl]-2-(2-thienyl)benzoxazole. The yield was 70%. Recrystallization from ethyl acetate-hexane gave colorless prisms, mp 97-98° C.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06211215B1 |
| 출처 데이터셋 | uspto-grants-2001_04 |
| ORD ID | ord-d070bcd1c4a9497d8ba8cac2d29dda97 |
| 출처 메모 | uspto-grants-2001_04 |