Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
2-Acetylnaphthalene → N-[1-(2-naphthyl)ethyl]-1-(3-methoxyphenyl)ethylamine
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 2-Acetylnaphthalene | HCID 7122 | — |
| 반응물 | 1-(3-Methoxyphenyl)ethanamine | HCID 4612058 | — |
| 촉매 | Titanium isopropoxide | HCID 11026 | — |
| 생성물 | N-[1-(2-naphthyl)ethyl]-1-(3-methoxyphenyl)ethylamine | HCID 22011059 | — |
반응 단계
In a similar fashion equal molar amounts 1-(3-methoxyphenyl)ethylamine (1.51 g, 10 mmol), 2′-acetonaphthone (1.70 g, 10 mmol) and 1.25 equivalents of titanium(IV) isopropoxide (3.55 g, 12.5 mmol) were treated as above. Work-up yielded N-[1-(2-naphthyl)ethyl]-1-(3-methoxyphenyl)ethylamine, 6F, as a clear, colorless oil; m/z (rel. int.) 305 (M+, 1), 290 (35), 170 (49), 155 (100), 135 (55), 115 (8), 105 (10), 91 (9), 77 (10).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06211244B1 |
| 출처 데이터셋 | uspto-grants-2001_04 |
| ORD ID | ord-4464b040a8584a058b6e9f2f05b92b04 |
| 출처 메모 | uspto-grants-2001_04 |