Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Benzenepropanoyl chloride → N-(3-phenylpropionyl)-D,L-alanine Isobutyl Ester
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Benzenepropanoyl chloride | HCID 64801 | — |
| 반응물 | 2-Methylpropyl 2-aminopropanoate hydrochloride | HCID 86200109 | — |
| 생성물 | N-(3-phenylpropionyl)-D,L-alanine Isobutyl Ester | HCID 15480461 | — |
반응 단계
Following General Procedure A′ above and using 3-phenylpropionyl chloride (Aldrich) and D,L-alanine iso-butyl ester hydrochloride (from Example B′ above), the title compound was prepared as a solid having a melting point of from 51°-54° C. The reaction was monitored by tlc on silica gel and purification was by extraction with Et2O followed by washes with aqueous K2CO3 and aqueous HCl.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06211235B1 |
| 출처 데이터셋 | uspto-grants-2001_04 |
| ORD ID | ord-2dcf518fab9749e9a6a7476a3fdeee2d |
| 출처 메모 | uspto-grants-2001_04 |