Formic Acid → 1-Cyano-1-formylaminocyclopentane

HRID 322811

반응식

HRID 322811 반응식
[NH2:1][C:2]1([C:7]#[N:8])[CH2:6][CH2:5][CH2:4][CH2:3]1.[CH:9](O)=[O:10]>O>[C:7]([C:2]1([NH:1][CH:9]=[O:10])[CH2:6][CH2:5][CH2:4][CH2:3]1)#[N:8]

참가 물질

4

반응물 2

HCID 284Formic AcidHCID 21068971-Aminocyclopentanecarbonitrile

생성물 1

HCID 212029501-Cyano-1-formylaminocyclopentane

시약·촉매·용매 1

HCID 962Water용매

실험 절차

11.0 g (0.1 mol) of 1-amino-1-cyanocyclopentane and 10 ml of 85% formic acid were placed in an apparatus equipped with water-separatory distillation head and boiled for 3 hours. The reaction mixture was then evaporated to constant weight in vacuo.

후처리

  1. customThe reaction mixture was then evaporated to constant weight in vacuo

출처 및 근거

ORD 기록
ord-def3b84f363245bdb19ba349862925db
출처 데이터셋
uspto-grants-2001_04
특허 번호
US06211382B1

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