Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
3-Bromophenyl isocyanate → N-(2-hydroxy-4-nitrophenyl)-N'-(3-bromophenyl)urea
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 3-Bromophenyl isocyanate | HCID 141001 | — |
| 반응물 | 2-Amino-5-Nitrophenol | HCID 4984721 | — |
| 생성물 | N-(2-hydroxy-4-nitrophenyl)-N'-(3-bromophenyl)urea | HCID 21184715 | 87% |
반응 단계
N-(2-Hydroxy-4-nitrophenyl)-N′-(3-bromo phenyl)urea was prepared from 2-hydroxy 4-nitro aniline (500 mg, 3.24 mmol) and 3-bromo phenyl isocyanate (3.24 mmol) according to the procedure in General Method B. The product was purified by dilution with methylene chloride and precipitation with hexanes. Filtering afforded the title compound (0.96 g, 87%). EI-MS m/z 350 (M−H)−
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06211373B1 |
| 출처 데이터셋 | uspto-grants-2001_04 |
| ORD ID | ord-ee8cb439a0e8475ab05b9bfca1497727 |
| 출처 메모 | uspto-grants-2001_04 |